超临界CO2流体萃取法和水蒸汽蒸馏法提取山柰挥发油化学成分的研究

超临界CO2流体萃取法和水蒸汽蒸馏法提取山柰挥发油化学成分的研究

邱琴¹,杨厚玲²,陈士恒¹,陈婷婷¹,韩玲³,刘廷礼¹

1. 山东大学环境科学与工程学院，山东济南250100； 2. 济南职业学院工商管理系，山东济南250014；3. 山东大学化学与化工学院，山东济南250100

收稿日期:2006-05-29 修回日期:1900-01-01 出版日期:2006-10-24 发布日期:2006-10-24
通讯作者: 邱琴

Chemical constituents for the essential oil ofKaempferia.galanga L by supercritical fluid extraction and stem distillation

QIU Qin,CHEN Ting-ting,HAN Ling,LIU Ting-li,

1. School of Environmental Science and Engineering, Shandong Univ., Jinan 250100， Shandong, China;2. Department of Business Administration， Jinan Vocational College, Jinan 250014, Shandong, China;

Received:2006-05-29 Revised:1900-01-01 Online:2006-10-24 Published:2006-10-24

摘要/Abstract

摘要： 采用超临界CO2流体萃取法(SFE)与水蒸气蒸馏法(SD)从山柰中提取挥发油. 用气相色谱质谱联用技术对化学成分进行分析，用归一化法测定其相对百分含量. 超临界CO2流体萃取法提取的挥发油共鉴定了39种成分，占挥发油总成分的86％以上；水蒸气蒸馏法提取的挥发油共鉴定了51种成分，占挥发油总成分的89％以上. 研究表明超临界CO2流体萃取法提取的挥发油能更真实、全面地反映药材中的化学成分.

关键词: 山柰, 超临界流体萃取, 气相色谱-质谱 , 水蒸气蒸馏

Abstract: Essential oil was extracted from Kaempferia.galanga L by supercritical fluid extraction (SFE) and steam distillation (SD). The extracted components were determined by gas chromatography with area normalization method, and were identified by gas chromatographymass spectrometry. There are 39 components separated and identified from Kaempferia.galanga L by SFE, which compose of about 86% of the total essential oil. There are 51 components seperated and identified from Kaempferia.galanga L by SD, which compose of about 89% of the total essential oil. The result shows that SFE method can reflect the chemical components of the medicinal materials more accurately and more comprehensively.

Key words: GCMS0 , steam distillation, supercritical fluid extraction, Kaempferia.galanga L

邱琴,杨厚玲,陈士恒,陈婷婷,韩玲,刘廷礼 . 超临界CO2流体萃取法和水蒸汽蒸馏法提取山柰挥发油化学成分的研究[J]. J4, 2006, 41(6): 119-123 .

QIU Qin,CHEN Ting-ting,HAN Ling,LIU Ting-li, . Chemical constituents for the essential oil ofKaempferia.galanga L by supercritical fluid extraction and stem distillation[J]. J4, 2006, 41(6): 119-123 .

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